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Capping layers for Al
Capping layers for AlEdit

    Al 100 / Ti 20 / Pd 5

    On standard Si <100> 300µm / SiO2 500nm

    • evap Old Plassys
    Al 100nm @ 1nm/s, P_ev = 5e-7
    Ti 2*10nm @ 0.5nm/s (error on evap, make a skip step at 10nm, have to relaunch)
    Pd 5nm @ 0.2nm/s (wait about 10min, because I initially don't have rights to use Pd)
    
    • observation

    No apparent default on optical microscope (no tiny black spots)

    Al100-Ti20-Pd5_init.JPG

    • etch rate in MIF726

    Let it for 15', see no effect

    • etch rate in MF319

     

    • Contact resistance without Ion beam (WJOX1_10)

    WJOX1_10_sem.jpg
    oxidation 24h at ambient
    contacts are in between 57Ω and 75Ω
     

    • SEM observation

    bare, aged 200°C 2h,

    • Tc measurement

     

    • RF measurement
    Summary
    sample oxy  (h) etch time (s) evap RA (Ω) SA
    10-3µm2
    nb sq A RB (Ω) SB 10-3µm2 nb sq B RC (Ω) SC 10-3µm2 nb sq C RD (Ω) SD 10-3µm2 nb sq D average
    Rcontact (Ω*µm2)
    sheet resistance
    (Ω/□)
    comment
    WJOX1_10 24 0 old/old 90 9 25 56.7 9 17 59.3 113 20 74.2 41 20     Al20/Ti10/Pd5 // Al60
                                         
    Al 150 / Pd 5

    On Si:B <100> 300µm, rho~3-4kohm.cm (lot 2451)

    • evap Old Plassys
    Al 150nm @ 1nm/s, P_ev = 5e-7
    Pd 5nm @ 0.2nm/s 
    • etch rate in MIF726

    Etched in ~15'. Leaves the Pd peel on the wafer.

    • etch rate in MF319

    Etched in ~13'. Leaves the Pd peel on the wafer.

    • Tc measurement

     

    • RF measurement
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